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B5柴油
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GB 25199-2017
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标准编号: GB 25199-2017 (GB25199-2017)
中文名称: B5柴油
英文名称: B5 diesel fuels
行业: 国家标准
中标分类: E31
字数估计: 17,139
发布日期: 2017-09-07
实施日期: 2017-09-07
旧标准 (被替代): GB 25199-2015; GB/T 20828-2015
起草单位: 中国石油化工股份有限公司石油化工科学研究院
归口单位: 全国石油产品和润滑剂标准化技术委员会(SAC/TC 280)
提出机构: 国家能源局
发布机构: 中华人民共和国国家质量监督检验检疫总局、中国国家标准化管理委员会
GB 25199-2017: B5柴油
GB 25199-2017 英文名称: B5 diesel fuels
1 范围
本标准规定了由BD100生物柴油和石油柴油调合的B5柴油的术语和定义、分类和标记、要求和试
验方法、检验规则及标志、包装、运输和贮存及安全。
本标准适用于压燃式发动机使用的、以BD100生物柴油为调合组分的B5普通柴油和B5车用
柴油。
2 规范性引用文件
下列文件对于本文件的应用是必不可少的。凡是注日期的引用文件,仅注日期的版本适用于本文
件。凡是不注日期的引用文件,其最新版本(包括所有的修改单)适用于本文件。
GB 190 危险货物包装标志
GB 252 普通柴油
GB/T 261 闪点的测定 宾斯基-马丁闭口杯法
GB/T 264 石油产品酸值测定法
GB/T 265 石油产品运动粘度测定法和动力粘度计算法
GB/T 268 石油产品残炭测定法(康氏法)
GB/T 386 柴油着火性质测定法(十六烷值法)
GB/T 508 石油产品灰分测定法
GB/T 510 石油产品凝点测定法
GB/T 511 石油产品和添加剂机械杂质测定法
GB/T 1884 原油和液体石油产品密度实验室测定法(密度计法)
GB/T 1885 石油计量表
GB/T 2433 添加剂和含添加剂润滑油硫酸盐灰分测定法
GB/T 4756 石油液体手工取样法
GB/T 5096 石油产品铜片腐蚀试验法
GB/T 5526 植物油脂检验 比重测定法
GB/T 5530 动植物油脂 酸值和酸度测定
GB/T 6536 石油产品蒸馏测定法
GB/T 6540 石油产品颜色测定法
GB/T 7304 石油产品酸值的测定 电位滴定法
GB/T 11140 石油产品硫含量的测定 波长色散X射线荧光光谱法
GB/T 12700 石油产品和烃类化合物 硫含量的测定 Wickbold燃烧法
GB/T 13377 原油和液体或固体石油产品 密度或相对密度的测定 毛细管塞比重瓶和带刻度
双毛细管比重瓶法
GB/T 17040 石油和石油产品硫含量的测定 能量色散X射线荧光光谱法
GB/T 17144 石油产品残炭测定法(微量法)
GB/T 17476 使用过的润滑油中添加剂元素、磨损金属和污染物以及基础油中某些元素测定法
(电感耦合等离子体发射光谱法)
GB 19147 车用柴油
GB/T 23801 中间馏分油中脂肪酸甲酯含量的测定 红外光谱法
GB/T 25963 含脂肪酸甲酯中间馏分芳烃含量的测定 示差折光检测器高效液相色谱法
GB 30000.7-2013 化学品分类和标签规范 第7部分:易燃液体
GB/T 33400 中间馏分油、柴油及脂肪酸甲酯中总污染物含量测定法
SH/T 0164 石油产品包装、贮运及交货验收规则
SH/T 0175 馏分燃料油氧化安定性测定法(加速法)
SH/T 0246 轻质石油产品中水含量测定法(电量法)
SH/T 0248 柴油和民用取暖油冷滤点测定法
SH/T 0253 轻质石油产品中总硫含量测定法(电量法)
SH/T 0604 原油和石油产品密度测定法(U型振动管法)
SH/T 0606 中间馏分烃类组成测定法(质谱法)
SH/T 0689 轻质烃及发动机燃料和其他油品的总硫含量测定法(紫外荧光法)
SH/T 0749 润滑油及添加剂中添加元素含量测定法(电感耦合等离子发射光谱法)
SH/T 0765 柴油润滑性评定法(高频往复试验机法)
SH/T 0796 B-100生物柴油脂肪酸甲酯中游离甘油和总甘油含量测定法(气相色谱法)
NB/SH/T 0825 脂肪酸甲酯氧化安定性的测定 加速氧化法
NB/SH/T 0831 生物柴油中脂肪酸甲酯及亚麻酸甲酯含量的测定 气相色谱法
NB/SH/T 0842 汽油和柴油中硫含量的测定 单波长色散X射线荧光光谱法
NB/SH/T 0873 生物柴油及其调合燃料氧化安定性的测定 加速氧化法
NB/SH/T 0916 柴油燃料中生物柴油(脂肪酸甲酯)含量的测定 红外光谱法
ASTMD4951 润滑油中添加剂元素测定法(电感耦合等离子体原子发射光谱法)
ASTMD7039 汽油和柴油中硫含量的测定 单波长色散 X射线荧光光谱法
ASTMD7111 中间馏分油中微量元素测定法[电感耦合等离子体原子发射光谱法
EN14107 油脂衍生物-脂肪酸甲酯(FAME)-磷含量测定法[电感耦合等离子体(ICP)发射光
谱法]
EN14538 油脂衍生物-脂肪酸甲酯(FAME)-Ca、K、Mg和Na含量测定法[电感耦合等离子体发
射光谱法
3 术语和定义
下列术语和定义适用于本文件。
3.1
BD100生物柴油
由动植物油脂或废弃油脂与醇(例如甲醇或乙醇)反应制得的脂肪酸单烷基酯,最典型的为脂肪酸
甲酯(FAME),以BD100表示。
3.2
石油柴油
由石油制取的,或加有添加剂的用于压燃式发动机的烃类液体燃料。
3.3
B5柴油
体积分数为1%~5%的BD100生物柴油与体积分数为95%~99%的石油柴油的调合燃料。
3.4
游离甘油
3.5
单甘酯
油脂或脂肪酸发生部分反应生成的甘油骨架上只有一个长侧链烷基的甘油酯。
3.6
总甘油
生物柴油中游离甘油与未反应或部分反应的动植物油脂甘油部分的总和。
4 分类和标记
4.1 产品分类
4.1.1 类别:本标准所属产品按用途分为B5普通柴油和B5车用柴油两个类别。B5普通柴油是体积
普通柴油的调合燃料,适用于拖拉机、内燃机车、工程机械、内河船舶和发电机组等压燃式发动机;B5车用柴油是体积分数为1%~5%的BD100生物柴油与体积分数为95%~99%的除润滑性外其余指标满
足GB 19147的车用柴油的调合燃料,适用于压燃式发动机汽车使用的以生物柴油为调合组分的车用
柴油。B5车用柴油又分为B5车用柴油(Ⅴ)和B5车用柴油(Ⅵ)。
注:可参见附录A,使用不同牌号的B5柴油。
GB 25199-2017
GB
NATIONAL STANDARD OF THE
PEOPLE’S REPUBLIC OF CHINA
ICS 75.160.20
E 31
Replacing GB 25199-2015, GB/T 20828-2015
B5 diesel fuels
B5柴油
ISSUED ON. SEPTEMBER 07, 2017
IMPLEMENTED ON. SEPTEMBER 07, 2017
Issued by. General Administration of Quality Supervision, Inspection and
Quarantine;
Standardization Administration of the People's Republic of
China.
Table of Contents
Foreword . 3
1 Scope .. 5
2 Normative references . 5
3 Terms and definitions . 8
4 Classification and marking .. 9
5 Requirements and test methods . 10
6 Inspection rules .. 14
7 Markings, packaging, transport and storage . 15
8 Safety . 15
9 Standard implementation . 16
Appendix A (Informative) Lowest temperature in each region with a risk of 10%
. 17
Appendix B (Normative) Test of nitrate cetane number improver in diesel .. 19
Appendix C (Normative) BD100 Biodiesel . 22
Foreword
Clause 5 of this standard is mandatory, the rest are recommended.
This standard was drafted in accordance with the rules given in GB/T 1.1-2009.
This standard replaces GB 25199-2015 “Biodiesel fuel blends (B5)” and GB/T
20828-2015 “Biodiesel blend stock (BD100) for diesel engine fuels”.
As compared with GB 25199-2015 and GB/T 20828-2015, the main technical
changes of this standard are as follows.
- COMBINE these two standards, CHANGE the name to “B5 diesel fuels”;
- DELETE the technical requirements and test methods of B5 vehicle diesel
(IV);
- ADD the technical requirements and test methods of B5 vehicle diesel (VI);
- INCLUDE the content of GB/T 20828-2015 as Appendix C of this standard.
As compared with GB/T 20828-2015, the main technical changes in Appendix
C of this standard are as follows.
- MODIFY the name from “Biodiesel blend stock (BD100) for diesel engine
fuels” to “BD100 Biodiesel”;
- MODIFY the closed flash point from not less than 101 °C to not less than
130 °C;
- CANCEL the methanol content indicator;
- CANCEL the 90% recovery temperature indicator.
This standard was proposed by the National Energy Administration.
This standard shall be under the jurisdiction of the National Standardization
Technical Committee for Petroleum Products and Lubricants (SAC/TC 280).
Drafting organizations of this standard. China Petroleum & Chemical
Corporation Petrochemical Research Institute.
The main drafters of this standard. Lin Jianmin, Li Baoshi, Huang Yanmin,
Zhang Jianrong, Liu Jinsheng, Gao Lan.
This standard replaces the standard previously issued as follows.
- GB/T 20828-2007, GB/T 20828-2014, GB/T 20828-2015;
B5 diesel fuels
Warning - If it does not take appropriate precautionary measures, the
product to which this standard belongs may be hazardous during
production, transportation, handling, storage, transportation, and use.
This standard is not intended to suggest all safety issues related to this
product. Users are responsible for adopting appropriate safety and
preventive measures and ensuring compliance with the conditions
stipulated by relevant national laws and regulations.
1 Scope
This standard specifies the terms and definitions, classifications and markings,
requirements and test methods, inspection rules and markings, packaging,
and petroleum diesel.
This standard is applicable to B5 common diesel fuel and B5 motor vehicle
diesel fuel used in compression-combustion engines with BD100 biodiesel as
the blending component.
2 Normative references
The following documents are essential to the application of this document. For
the dated documents, only the versions with the dates indicated are applicable
to this document; for the undated documents, only the latest version (including
all the amendments) are applicable to this standard.
GB 252 General diesel fuels
GB/T 261 Determination of flash point - Pensky-Martens closed cup method
GB/T 264 Petroleum products - Determination of acid number
GB/T 265 Petroleum products - Determination of kinematic viscosity and
calculation of dynamic viscosity
GB/T 268 Petroleum products - Determination of carbon residue -
Conradson method
GB/T 386 Standard test method for cetane number of diesel fuel oil
GB/T 508 Petroleum products - Determination of ash
GB/T 511 Petroleum products and additives - Determination of mechanical
impurities-Gravimetric method
GB/T 1884 Crude petroleum and liquid petroleum products - Laboratory
determination of density - Hydrometer method
GB/T 1885 Petroleum measurement tables
GB/T 2433 Petroleum products - Lubricating oils and additives -
Determination of sulfated ash
GB/T 4756 Method for manual sampling of petroleum liquids
GB/T 5096 Test method for corrosiveness to copper from petroleum products
GB/T 5526 Inspection of vegetable oils - Methods for determination of
specific gravity
GB/T 5530 Animal and vegetable fats and oils - Determination of acid value
and acidity
GB/T 6536 Standard test method for distillation of petroleum products at
atmospheric pressure
GB/T 6540 Petroleum products - Determination of color
GB/T 7304 Standard test method for acid number of petroleum products by
potentiometric titration
wavelength dispersive X-ray fluorescence spectrometry
GB/T 12700 Petroleum products and hydrocarbons - Determination of sulfur
content - Wickbold combustion method
GB/T 13377 Crude petroleum and liquid or solid petroleum products -
Determination of density or relative density-Capillary stoppered pyknometer
and graduated bicapillary pyknometer methods
GB/T 17040 Standard test method for sulfur in petroleum and petroleum
products by energy dispersive X-ray fluorescence spectrometry
GB/T 17144 Petroleum products - Determination of carbon residue - Micro
SH/T 0765 Diesel fuel - Assessment of lubricity using the high-frequency
reciprocating rig (HFRR)
SH/T 0796 Test method for determination of free and total glycerine in B-100
biodiesel methyl esters by gas chromatography
NB/SH/T 0825 Standard test method for determination of oxidation stability
of fatty acid methyl ester by accelerated oxidation test
NB/SH/T 0831 Test method for determination of fatty acid methyl esters and
linolenic acid methyl ester contents in biodiesel by gas chromatography
NB/SH/T 0842 Standard test method for sulfur in gasoline and diesel fuel by
NB/SH/T 0873 Determination of oxidation stability of biodiesel fuel and its
blending fuel - Accelerated oxidation method
NB/SH/T 0916 Determination of biodiesel (fatty acid methyl esters) content
in diesel fuels - Infrared spectroscopy
ASTM D4951 Standard test method for determination of additive elements
in lubricating oils by inductively coupled plasma atomic emission
spectrometry
ASTM D7039 Standard test method for sulfur in gasoline and diesel fuel by
monochromatic wavelength dispersive X-ray fluorescence spectrometry
middle distillate fuels by inductively coupled plasma atomic emission
spectrometry (ICP-AES)
EN14107 Fat and oil derivatives - Fatty acid methyl ester (FAME) -
Determination of phosphorus content by inductively coupled plasma (ICP)
emission spectrometry
EN14538 Fat and oil derivatives - Fatty acid methyl ester (FAME) -
Determination of Ca, K, Mg and Na content by optical emission spectral
analysis with inductively coupled plasma (ICP OES)
3 Terms and definitions
3.1
BD100 biodiesel
b) When there are significant changes have taken place in raw materials and
processes, which may affect product quality;
c) When there is significant difference between the results of the exit-factory
inspection or periodic inspection and the results of the last type inspection.
6.2 Batching
Under the condition of unchanged raw materials and processes, each tank of
kettle of products are considered as one batch.
Sampling is made in accordance with GB/T 4756, 4 L sample is taken for
inspection and retention.
6.4 Judgment rules
When the results of the exit-factory inspection meet all the technical
requirements in Table 1, Table 2 or Table 3 of this standard, the batch of
products is determined to be qualified.
6.5 Re-inspection rules
If the exit-factory inspection results do not meet the technical requirements of
Table 1, Table 2 or Table 3, double-quantity of samples shall be taken from the
perform re-inspection for the unqualified items. If the re-inspection result still
does not meet the specified technical requirements, the batch of products shall
be judged as unqualified.
7 Markings, packaging, transport and storage
7.1 The dispensers used for B5 diesel oil which is sold to users that meet the
requirements of Table 1, Table 2 and Table 3 of this standard shall clearly
indicate the name, designation and grade (V or VI) of the product, such as No.0
B5 general diesel, No. 0 B5 vehicle diesel (V), etc.
7.2 B5 diesel is a flammable liquid. The marking, packaging, transportation and
with SH/T 0164, GB 30000.7-2013 and GB 190.
8 Safety
B5 diesel is a flammable liquid. Please refer to Appendix D of GB 30000.7-2013
for the hazard description and precautionary statements.
Appendix B
(Normative)
Test of nitrate cetane number improver in diesel
B.1 Scope
This method is sui...
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